Beilstein J. Org. Chem.2015,11, 265–270, doi:10.3762/bjoc.11.29
been achieved in twelve steps. By comparison of the NMR spectra of the synthesized compounds with those of the natural products, a relative stereochemistry is suggested, especially that of the ketal carbon.
Keywords: acylphloroglucinols; bicyclisation; furo[2,3-b]chromene; fusedketal; Introduction
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Graphical Abstract
Figure 1:
Hyperaspidinols A (1) and B (2) and other compounds 3-6 from Hypericum chinense.